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3550B Datasheet(PDF) 3 Page - 3M Electronics

Part # 3550B
Description  Scotch-WeldTM Structural Void Filling Compound
PDF  8 Pages
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Manufacturer  3M [3M Electronics]
Direct Link  http://www.3m.com
Logo 3M - 3M Electronics

3550B Datasheet(HTML) 3 Page - 3M Electronics

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3M™ Scotch-Weld™
Structural Void Filling Compound 3550 B/A FST
Technical Datasheet
- 3 -
Typical Product Performance
Note: The following technical information and data should be considered representative or typical only and should
not be used for specification purposes. The following mechanical and physical data is based on Scotch-Weld
3550 B/A FST Compound.
Physical Properties
Thermal expansion:
The low-density void-filler was manually mixed and carefully filled into mold with inner dimensions of
approximately 2" x 2" x 8" (50 x 50 x 200 mm). Filler block was cured 14 days at 74°F (23 ± 2°C). The block
was machine milled into 20 individual specimens of dimensions 0.3” x 0.3” x 0.6” (7 x 7 x 15 mm) with a
tolerance of ± 0.004" (± 0.1 mm). The coefficient of thermal expansion (C.T.E.) was then determined per ASTM
E-831 test method using a PerkinElmer® thermo-mechanical analyzer (PerkinElmer, Waltham, MA).* After cold
stabilization at -40°F (- 40°C), three specimens of each lot were scanned at a rate of 2°C/min from -40°F to
392°F (-40°C to 200°C). The coefficient of thermal expansion was determined on the two linear portions of the
curve below and above the glass transition temperature of the product.
Exothermicity:
Round cups were filled with approximately 3.5 oz (100 grams) of the void-filler. A thermocouple was placed in the
center of the void-filler. Cure cycle is 74°F (23 ± 2°C) during 14 hours.
Cured density:
The cured density was determined on individual specimens cut from a cured block of void-filler with a band saw.
The density was calculated by dividing the mass of the specimen by its measured volume. The density was
expressed in g/cc.
Volatiles test:
Approximately 1 oz (30 grams) of the void-filler was spread onto a circular surface of a metal pan having a
diameter of about 3.3" or 85 mm. After weighing the specimens, they were cured 48h @ 74°F (23 ± 2°C) and
then reweighed.
Properties
Test Method
Average
Thermal Expansion
ASTM E-831
1.1E-04 /°C @ 14 to 176°F (-10 to 80°C)
1.4E-04 /°C @ 176 to 410°F (80 to 210°C)
Extrudability
AITM 7-0003 (B) (see 4.3.8.6)
3.0 oz/min (85 g/min)
Exothermicity
AIMS 10-03-000 (4.2.8.3) ∆T
7.5°F (4.5°C)
Cured Density
ISO 1183
0.57 ± 0.05 g/cc
Volatile Content
AIMS 10-03-000 (4.2.8.1)
0.03 %
DSC Scan:
Tooling
• DSC Q2000 from TA Instruments with auto sampler and RCS cooling system.
• Two point calibration with Indium and water.
• The sample head was flushed with nitrogen gas, 25ml/min purge rate.
Sample Preparation
For the measurement of the fresh mixed sample: part of the fresh mixed paste was weighed into a hermetic Al
pan. The rest of the mixed paste was stored at RT in the lab and used for the measurement after 2 days & 7 days.
For these samples: parts of the hard brittle material was cut out and weighed on an Al pan with holes in the lid.
Program Steps
(1) Equilibrate at -50°C
(5) Isothermal for 10 min
(2) Ramp 10°C/min to 250°C
(6) Mark end of cycle 1
(3) Mark end of cycle 0
(7) Ramp 10°C/min to 250°C
(4) Ramp 20°C/min to -50°C
(8) Mark end of cycle 2



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